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The stability of organic solvents and carbon electrode in nonaqueous Li-O2 batteries
May 21 , 2021
2. Experimental 2.1. Preparation and cell testing Ethylene carbonate (EC), propylene carbonate (PC), DME,tri(ethylene glycol) dimethyl ether (i.e., Triglyme), di(ethyleneglycol) di-n-butyl ether (i.e. butyl diglyme, BDG), and lithiumbis(trifluoromethylsulfonyl)imide (LiTFSI) (all in batterygrade) were purchased from Novolyte Technologies. DMSO,triethyl phosphate (TEPa), 1-butyl-1-methylpyrrolidium...
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Air Dehydration Membranes for Nonaqueous Lithium–Air Batteries
May 28 , 2021
Jian Zhang, Wu Xu,* Xiaohong Li, and Wei Liuz PTFE thin film coated on the porous metal substrate sheet.— In the third stage of our membrane development, the PTFE membranes were coated onto the metal substrates by spin coating with DuPont PTFE TE-3859 fluoropolymer resin. The resin is anegatively charged, hydrophobic colloid containing approximately60% by total weight of 0.05–0.5 m PTFE particles ...
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Solvent-Free Dry Powder Coating Process for Low-Cost Manufacturing of LiNi1/3Mn1/3Co1/3O2 Cathodes in Lithium-Ion Batteries
Jun 04 , 2021
Mohanad Al-Shroofy,aQinglin Zhang,aJiagang Xu,aTao Chen,aAman Preet Kaur,band Yang-Tse Chenga 2. Experimental 2.1 Electrode Fabrication 2.1.1 Dry-Powder-Coated Electrodes.To prepare the dry cathode mixture, NMC (Umicore) was mixed with carbon black (CB, Super P C65, TIMCAL) in a planetary mixer-deaerator (Mazerustar KK-50S, Kurabo) for 20 min. The NMC particle size is between 5.6 µm and 12 µm (D50...
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Synthesis, characterization, and evaluation of unsupported porous NiS submicrometer spheres as a cathode material for lithium batteries
Jun 18 , 2021
Debajyoti Mondal•Gilles Villemure•Chaojie Song 2.2 Synthesis of porous NiS submicrospheres The USP procedure for the synthesis of nanomaterials wasreported elsewhere [54]. A solution containingNiCl26H2O, Na2S2O35H2O, and colloidal silica was prepared according to a procedure reported in our previouspaper [55]. The solution was loaded to a USP ultrasonic cell, after which the system was purged with...
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The Influence of Polyvinylidene Fluoride (PVDF) Binder Properties on LiNi0.33Co0.33Mn0.33O2(NMC) Electrodes Made by a Dry-PowderCoating Process
Jun 21 , 2021
To cite this article: Ming Wang et al 2019 J. Electrochem. Soc. 166 A2151 Preparation of electrodes.—A manually operated powder coatingspray gun (Encore LT Manual Powder Coating System, Nordson) was used for the ESD process. One piece of 16μm thick aluminum foil was used as the electrode substrate, one piece of electrically grounded Cuplate (250μm thick) was used as the platform. The operation vol...
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An Approach to Make Macroporous Metal Sheets as Current Collectors for Lithium-Ion Batteries
Jun 23 , 2021
The freestanding, laminated film was sintered in air by increasing the temperature of the furnace at a slow rate to 1000°C, holding at1000°C for 1 h, and then decreasing the temperature at a rate of5°C/min to room temperature. This high temperature treatment was done to completely burn all carbon and organic materials to generate a porous structure and to simultaneously allow CuO particles to conn...
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Effects of the Mixing of an Active Material and a Conductive Additive on the Electric Double Layer Capacitor Performance in Organic Electrolyte
Jun 25 , 2021
2. Experimental Procedure Activated carbon(MSP-20) for an active electrode material was provided from Kansai Coke & Chemicals Co.. Super-P(M.M.M. Carbon Co., Belgium) and polyvinylidene fluoride(Sigma-Aldrich) were employed as a conductive additive and a binder, respectively. The preparation procedure for a coin-type EDLC cell was briefly presented in Fig. 1. Active materia...
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Monolithic Nanoporous Zn Anode for Rechargeable Alkaline Batteries
Jun 28 , 2021
Congcheng Wang,# Guoyin Zhu,# Pan Liu, and Qing Chen* METHODS Battery Assembly and Testing. Ni−Zn batteries were assembled into coin-type cells (CR2032) with a Zn anode, either the compressed nanoporous Zn (∼0.36 cm2 in size) or a pasted electrode comprising Zn powder (90 wt %, Aldrich), polyvinylidene fluoride (Arkema Kynar), and a NiOOH cathode (650 mAh, GP Batteries). Tin foil was used as the a...
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Effect of entropy change of lithium intercalation in cathodes and anodes on Li-ion battery thermal management
Jun 30 , 2021
Vilayanur V. Viswanathan∗, Daiwon Choi, Donghai Wang11, Wu Xu, Silas Towne, Ralph E. Williford, Ji-Guang Zhang, Jun Liu, Zhenguo Yang 3. Experiment 3.1. Electrode synthesis Nanosized LiFePO4 was synthesized using LiCoOCH3•2H2O(reagent grade, Sigma), FeCO2•2H2O (99%, Aldrich), (NH4)H2PO4(99.999%, Sigma–Aldrich), oleic acid (FCC, FG) and paraffin wax(ASTM D 87, mp. 53–57◦C, Aldrich). (NH4)H2PO4 was ...
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